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Yıl 2021, , 253 - 303, 17.05.2021
https://doi.org/10.15671/hjbc.815414

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Chiral Separations by Capillary Electrophoresis and related Techniques with Different Chiral Selectors: A Review

Yıl 2021, , 253 - 303, 17.05.2021
https://doi.org/10.15671/hjbc.815414

Öz

Kiral bileşiklerin tanınma mekanizması ve enantiyomerik olarak ayrılması, hem analitik saflık hem de büyük ölçekli çalışmalar için çözüm bulmakla ilgilenen farmakoloji ve doğa bilimlerindeki araştırmacıların büyük ilgisini her zaman uyandıran konulardır. Kapiler Elektroforez, kiral selektörlerin yüksek çözünürlüğü ve yüksek verimliliği gibi üstün özellikleri nedeniyle enantiyomerik ayırımlar için en önemli analitik yaklaşımlardan biri haline gelmiştir. Araştırmacıların ilgi göstermeye devam ettiği bu alanda, teknolojinin ve farklı formdaki kiral selektörlerin gelişim sürecine paralel olarak Kapiler Elektroforez felsefesi temelinde geliştirilen yeni tekniklerin varlığıyla gün geçtikçe gelişmeler ilerlemektedir. Bu derlemede, kapiler elektroforez ve bununla ilişkili teknikler hakkında bazı tanımlayıcı teorik bilgilerin yanı sıra, moleküler baskılanmış polimerler, siklodekstrinler, metal-organik kafesler, iyonik sıvılar, monolitler ve nanopartiküller gibi farklı kiral selektörler kullanılarak kiral ayırmalar üzerine yaklaşık son 10 yıldaki (2010-2020) çalışmalar derlenmiştir.

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  • 325. C. Aydogan, A. Denizli, Electrochromatographic Enantioseparation of Amino Acids Using Polybutylmethacrylate-based Chiral Monolithic Column by Capillary Electrochromatography, Chirality, 24 (2012) 606–609.
  • 326. C. Aydoğan, Z. El Rassi, Monolithic stationary phases with incorporated fumed silica nanoparticles. Part I. Polymethacrylate-based monolithic column with incorporated bare fumed silica nanoparticles for hydrophilic interaction liquid chromatography, J. Chromatogr. A, 1445 (2016) 55–61.
  • 326. C. Aydoğan, Z. El Rassi, Monolithic stationary phases with incorporated fumed silica nanoparticles. Part I. Polymethacrylate-based monolithic column with incorporated bare fumed silica nanoparticles for hydrophilic interaction liquid chromatography, J. Chromatogr. A, 1445 (2016) 55–61.
  • 327. C. Aydoğan, Z. El Rassi, Monolithic stationary phases with incorporated fumed silica nanoparticles. Part II. Polymethacrylate-based monolithic column with “covalently” incorporated modified octadecyl fumed silica nanoparticles for reversed-phase chromatography, J. Chromatogr. A, 1445 (2016) 62–67.
  • 327. C. Aydoğan, Z. El Rassi, Monolithic stationary phases with incorporated fumed silica nanoparticles. Part II. Polymethacrylate-based monolithic column with “covalently” incorporated modified octadecyl fumed silica nanoparticles for reversed-phase chromatography, J. Chromatogr. A, 1445 (2016) 62–67.
  • 328. S. Xu, R. Mo, C. Jin, X. Cui, R. Bai, Y. Ji, Mesoporous silica nanoparticles incorporated hybrid monolithic stationary phase immobilized with pepsin for enantioseparation by capillary electrochromatography, J. Pharm. Biomed. Anal., 140 (2017) 190–198.
  • 328. S. Xu, R. Mo, C. Jin, X. Cui, R. Bai, Y. Ji, Mesoporous silica nanoparticles incorporated hybrid monolithic stationary phase immobilized with pepsin for enantioseparation by capillary electrochromatography, J. Pharm. Biomed. Anal., 140 (2017) 190–198.
  • 329. C. Miao, R. Bai, S. Xu, T. Hong, Y. Ji, Carboxylated single-walled carbon nanotube-functionalized chiral polymer monoliths for affinity capillary electrochromatography, J. Chromatogr. A, 1487 (2017) 227–234.
  • 329. C. Miao, R. Bai, S. Xu, T. Hong, Y. Ji, Carboxylated single-walled carbon nanotube-functionalized chiral polymer monoliths for affinity capillary electrochromatography, J. Chromatogr. A, 1487 (2017) 227–234.
  • 330. Y. Li, X. Lin, S. Qin, L. Gao, Y. Tang, S. Liu, Y. Wang, β‐Cyclodextrin‐modified covalent organic framework as chiral stationary phase for the separation of amino acids and β‐blockers by capillary electrochromatography, Chirality, 32 (2020) 1008-1019.
  • 330. Y. Li, X. Lin, S. Qin, L. Gao, Y. Tang, S. Liu, Y. Wang, β‐Cyclodextrin‐modified covalent organic framework as chiral stationary phase for the separation of amino acids and β‐blockers by capillary electrochromatography, Chirality, 32 (2020) 1008-1019.
Toplam 660 adet kaynakça vardır.

Ayrıntılar

Birincil Dil İngilizce
Konular Mühendislik
Bölüm Articles
Yazarlar

Koray Şarkaya 0000-0003-0177-5134

İlgim Göktürk 0000-0001-7292-7241

Fatma Yılmaz 0000-0003-3260-1639

Adil Denizli 0000-0001-7548-5741

Yayımlanma Tarihi 17 Mayıs 2021
Kabul Tarihi 26 Aralık 2020
Yayımlandığı Sayı Yıl 2021

Kaynak Göster

APA Şarkaya, K., Göktürk, İ., Yılmaz, F., Denizli, A. (2021). Chiral Separations by Capillary Electrophoresis and related Techniques with Different Chiral Selectors: A Review. Hacettepe Journal of Biology and Chemistry, 49(3), 253-303. https://doi.org/10.15671/hjbc.815414
AMA Şarkaya K, Göktürk İ, Yılmaz F, Denizli A. Chiral Separations by Capillary Electrophoresis and related Techniques with Different Chiral Selectors: A Review. HJBC. Mayıs 2021;49(3):253-303. doi:10.15671/hjbc.815414
Chicago Şarkaya, Koray, İlgim Göktürk, Fatma Yılmaz, ve Adil Denizli. “Chiral Separations by Capillary Electrophoresis and Related Techniques With Different Chiral Selectors: A Review”. Hacettepe Journal of Biology and Chemistry 49, sy. 3 (Mayıs 2021): 253-303. https://doi.org/10.15671/hjbc.815414.
EndNote Şarkaya K, Göktürk İ, Yılmaz F, Denizli A (01 Mayıs 2021) Chiral Separations by Capillary Electrophoresis and related Techniques with Different Chiral Selectors: A Review. Hacettepe Journal of Biology and Chemistry 49 3 253–303.
IEEE K. Şarkaya, İ. Göktürk, F. Yılmaz, ve A. Denizli, “Chiral Separations by Capillary Electrophoresis and related Techniques with Different Chiral Selectors: A Review”, HJBC, c. 49, sy. 3, ss. 253–303, 2021, doi: 10.15671/hjbc.815414.
ISNAD Şarkaya, Koray vd. “Chiral Separations by Capillary Electrophoresis and Related Techniques With Different Chiral Selectors: A Review”. Hacettepe Journal of Biology and Chemistry 49/3 (Mayıs 2021), 253-303. https://doi.org/10.15671/hjbc.815414.
JAMA Şarkaya K, Göktürk İ, Yılmaz F, Denizli A. Chiral Separations by Capillary Electrophoresis and related Techniques with Different Chiral Selectors: A Review. HJBC. 2021;49:253–303.
MLA Şarkaya, Koray vd. “Chiral Separations by Capillary Electrophoresis and Related Techniques With Different Chiral Selectors: A Review”. Hacettepe Journal of Biology and Chemistry, c. 49, sy. 3, 2021, ss. 253-0, doi:10.15671/hjbc.815414.
Vancouver Şarkaya K, Göktürk İ, Yılmaz F, Denizli A. Chiral Separations by Capillary Electrophoresis and related Techniques with Different Chiral Selectors: A Review. HJBC. 2021;49(3):253-30.

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