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Kobalt Ferrit Nanoparçacıkların Sentezi, Karakterizasyonu ve Fotokataliz Uygulamaları:Farklı Çöktürücü Maddelerin ve Yöntemlerin Etkisi

Year 2023, Volume: 13 Issue: 1, 432 - 447, 01.03.2023
https://doi.org/10.21597/jist.1219411

Abstract

Bu çalışmada, birlikte çöktürme ve sol-jel yöntemleri ile hazırlanan kobalt ferrit
nanopartiküllerin yapısal ve fotokatalitik özellikleri üzerinde sentez yönteminin etkisine ilişkin
bir araştırma sunulmaktadır. Çöktürücü maddeler olarak sodyum hidroksit, potasyum hidroksit
ve amonyak, jelleştirici madde olarak sitrik asit kullanılmıştır. Elde edilen kobalt ferrit
fotokatalizörlerinin karşılaştırmalı özellikleri X-ışını kırınımı (XRD), Fourier dönüşümü
kızılötesi (FTIR) spektroskopisi, taramalı elektron mikroskobu (SEM) ve enerji dağılımlı X Işını
analizi (EDX) karakterizasyon teknikleri ile incelenmiştir. Numunelerin fotokatalitik aktiviteleri,
görünür bölge ışıması altında Kristal Viyolet (KV) ve Rhodamin B (RhB)'nin fotobozunması ile
değerlendirildi. Birlikte çöktürme yöntemiyle ve çöktürücü madde olarak amonyak kullanılarak
sentezlenen kobalt ferrit, diğer örneklerle karşılaştırıldığında daha üstün fotokatalitik aktivite
sergiledi. Amonyak çöktürücüsü ile sentezlenen kobalt ferrit, fotokatalitik bozunma verimleri
KV ve RhB için, 40 dakika ve 120 dakika sürelerden sonra sırasıyla %100 ve %91.2 olarak
belirlendi. Boyaların fotobozunmasının yalancı birinci dereceden kinetik modeli takip ettiği
bulundu. Amonyak çöktürücüsü ile sentezlenen kobalt ferrit, yalancı birinci dereceden hız
sabitleri KV ve RhB için sırasıyla 0.0847 ve 0.0205/dak olarak belirlendi.

References

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Synthesis, Characterization and Photocatalysis Applications of Cobalt Ferrite Nanoparticles: The Effect of Different Precipitating Agents and Methods

Year 2023, Volume: 13 Issue: 1, 432 - 447, 01.03.2023
https://doi.org/10.21597/jist.1219411

Abstract

In this study, a research on the effect of synthesis method on the structural and photocatalytic
properties of cobalt ferrite nanoparticles prepared by co-precipitation and sol-gel methods is
presented. Sodium hydroxide, potassium hydroxide and ammonia were used as precipitating
agents and citric acid was used as gelling agent. The comparative properties of the obtained
cobalt ferrite photocatalysts were investigated by X-ray diffraction (XRD), Fourier transform
infrared (FTIR) spectroscopy, scanning electron microscopy (SEM) and energy dispersive X-ray
analysis (EDX) characterization techniques. The photocatalytic activities of the samples were
evaluated by photodegradation of Crystal Violet (KV) and Rhodamine B (RhB) under visible
irradiation. cobalt ferrite synthesized by co-precipitation method and using ammonia as the
precipitant showed superior photocatalytic activity compared to other samples. Photocatalytic
degradation efficiencies of cobalt ferrite synthesized with ammonia precipitator were determined
as 100% and 91.2% for KV and RhB after 40 minutes and 120 minutes, respectively. The
photodegradation of the dyes was found to follow the pseudo-first-order kinetic model. The
pseudo-first order rate constants of cobalt ferrite synthesized with ammonia precipitator were
determined as 0.0847 ve 0.0205/min for KV and RhB, respectively

References

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  • Dehvari M., Babaei A.A., Esmaeili S., (2023). Amplification of oxidative elimination of atrazine by Ultrasound/ Ultraviolet–assisted Sono/Photocatalyst using a spinel cobalt ferrite–anchored MWCNT as peroxymonosulfate activator, Journal of Photochemistry & Photobiology, A: Chemistry 437, 114452.
  • Dutta, S., Gupta, B., Srivastava, S.K., Gupta, A.K. (2021). Recent advances on the removal of dyes from wastewater using various adsorbents: a critical review, Materials Advances, 2, 4497-4531. Gao W., Ran C., Wang M., Li L., Su Z., Yao X., (2016). The role of reduction extent of graphene oxide in the photocatalytic performance of Ag/AgX (X = Cl, Br)/rGO composites and the pseudo-second-order kinetics reaction nature of the Ag/AgBr system, Phys. Chem. Chem. Phys. 18, 18219-18226.
  • Hasan, I., Walia, S., Alharbi K.H., Khanjer, A.M., Alsalme, A., Khan, R.A. (2020) Multi-walled carbon nanotube coupled β-cyclodextrin/PANI hybrid photocatalyst for advance oxidative degradation of crystal violet, Journal of Molecular Liquids 317,114216-114226.
  • Jabbar, R., Sabeeh, S.H., Hameed A.M. (2020). Structural, dielectric and magnetic properties of Mn+2 doped cobalt ferrite nanoparticles, Journal of Magnetism and Magnetic Materials 494, 165726.
  • Jain R., Kumar S., Meena S.K., (2022). Precipitating agent (NaOH and NH4OH) dependent magnetic properties of cobalt ferrite nanoparticles, AIP Advances 12, 095109.
  • Jeseentharani, V., George, M., Jeyaraj, B., Dayalan, A., Nagaraja, K.S. (2013). Synthesis of metal ferrite (MFe2O4, M=Co, Cu, Mg, Ni, Zn) nanoparticles as humidity sensor materials, Journal of Experimental Nanoscience, 8(3), 358-370.
  • Joseph, C.G., Taufiq-Yap, Y.H., Musta, B., Sarjadi, M.S., Elilarasi, L., (2021). Application of Plasmonic Metal Nanoparticles in TiO2-SiO2 Composite as an Efficient Solar-Activated Photocatalyst: A Review Paper, Frontiers in Chemistry 8, 568063.
  • Karakaş, I.H., Karcıoğlu Karakaş, Z. (2022). The effects of heat treatment temperatures on photocatalytic activity of cobalt ferrite nanoparticles synthesised by microwave‐assisted combustion method, Coloration Technology.
  • Keleş Güner, E., İçer, F., Özdemir, A., Çağlar, B. (2021). Farklı ışık kaynakları altında kristal viyole boyar maddesinin kaolin-BiFeO3 nanokompozit üzerinde fotobozunması. Gümüşhane Üniversitesi Fen Bilimleri Dergisi, 11(3), 815-827.
  • Khanı A., Sohrabı M.R., Khosravı M., Davallo, M., (2013). Enhancing purification of an azo dye solution in nanosized zero-valent iron-ZnO photocatalyst system using subsequent semibatch packed-bed reactor, Turkısh Journal of Engineering and Environmental Sciences 37, 91-99.
  • Kızıltaş, H., Aydın, Ö. (2022). Removal of Orange G dye using peanut shells activated carbon: a green synthesis approach. International Journal of Environmental Analytical Chemistry, 1-21.
  • Kirankumar, V. S., & Sumathi, S. (2018). Photocatalytic and antibacterial activity of bismuth and copper co-doped cobalt ferrite nanoparticles. Journal of Materials Science: Materials in Electronics, 29(10), 8738-8746. Kurian, M., Nair, D.S., (2016). Effect of preparation conditions on Nickel Zinc Ferrite nanoparticles: A comparison between sol–gel auto combustion and co-precipitation methods, Journal of Saudi Chemical Society 20, 517–522.
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There are 53 citations in total.

Details

Primary Language Turkish
Subjects Chemical Engineering
Journal Section Kimya / Chemistry
Authors

Eda Keleş Güner 0000-0002-4421-1315

Early Pub Date February 24, 2023
Publication Date March 1, 2023
Submission Date December 15, 2022
Acceptance Date January 31, 2023
Published in Issue Year 2023 Volume: 13 Issue: 1

Cite

APA Keleş Güner, E. (2023). Kobalt Ferrit Nanoparçacıkların Sentezi, Karakterizasyonu ve Fotokataliz Uygulamaları:Farklı Çöktürücü Maddelerin ve Yöntemlerin Etkisi. Journal of the Institute of Science and Technology, 13(1), 432-447. https://doi.org/10.21597/jist.1219411
AMA Keleş Güner E. Kobalt Ferrit Nanoparçacıkların Sentezi, Karakterizasyonu ve Fotokataliz Uygulamaları:Farklı Çöktürücü Maddelerin ve Yöntemlerin Etkisi. J. Inst. Sci. and Tech. March 2023;13(1):432-447. doi:10.21597/jist.1219411
Chicago Keleş Güner, Eda. “Kobalt Ferrit Nanoparçacıkların Sentezi, Karakterizasyonu Ve Fotokataliz Uygulamaları:Farklı Çöktürücü Maddelerin Ve Yöntemlerin Etkisi”. Journal of the Institute of Science and Technology 13, no. 1 (March 2023): 432-47. https://doi.org/10.21597/jist.1219411.
EndNote Keleş Güner E (March 1, 2023) Kobalt Ferrit Nanoparçacıkların Sentezi, Karakterizasyonu ve Fotokataliz Uygulamaları:Farklı Çöktürücü Maddelerin ve Yöntemlerin Etkisi. Journal of the Institute of Science and Technology 13 1 432–447.
IEEE E. Keleş Güner, “Kobalt Ferrit Nanoparçacıkların Sentezi, Karakterizasyonu ve Fotokataliz Uygulamaları:Farklı Çöktürücü Maddelerin ve Yöntemlerin Etkisi”, J. Inst. Sci. and Tech., vol. 13, no. 1, pp. 432–447, 2023, doi: 10.21597/jist.1219411.
ISNAD Keleş Güner, Eda. “Kobalt Ferrit Nanoparçacıkların Sentezi, Karakterizasyonu Ve Fotokataliz Uygulamaları:Farklı Çöktürücü Maddelerin Ve Yöntemlerin Etkisi”. Journal of the Institute of Science and Technology 13/1 (March 2023), 432-447. https://doi.org/10.21597/jist.1219411.
JAMA Keleş Güner E. Kobalt Ferrit Nanoparçacıkların Sentezi, Karakterizasyonu ve Fotokataliz Uygulamaları:Farklı Çöktürücü Maddelerin ve Yöntemlerin Etkisi. J. Inst. Sci. and Tech. 2023;13:432–447.
MLA Keleş Güner, Eda. “Kobalt Ferrit Nanoparçacıkların Sentezi, Karakterizasyonu Ve Fotokataliz Uygulamaları:Farklı Çöktürücü Maddelerin Ve Yöntemlerin Etkisi”. Journal of the Institute of Science and Technology, vol. 13, no. 1, 2023, pp. 432-47, doi:10.21597/jist.1219411.
Vancouver Keleş Güner E. Kobalt Ferrit Nanoparçacıkların Sentezi, Karakterizasyonu ve Fotokataliz Uygulamaları:Farklı Çöktürücü Maddelerin ve Yöntemlerin Etkisi. J. Inst. Sci. and Tech. 2023;13(1):432-47.