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Calculation of Structural Parameters and Optical Constants of Size Dependent ZrO2 Nanostructures

Year 2024, Volume: 10 Issue: 1, 114 - 124, 30.04.2024

Gülsen Şahin Sultan Göktaş

Abstract

In this study, structural parameters and optical constants of size dependent zirconium dioxide (ZrO2) nanostructures were calculated. The effect of particle size was investigated on the calculated structural and optical parameters/constants. ZrO2 nanostructures were produced by chemical route. To change the grain size of the ZrO2 nanostructures, different annealing temperatures (450-550 oC) were applied. The x-ray diffraction (XRD), scanning electron microscope (SEM), and ultraviolet/visible region (UV-Vis) spectroscopy measurement results were used to calculate the structural and optical parameters/constants. The results of XRD measurement showed the ZrO2 nanostructures were crystallized in single tetragonal (cubic) ZrO2 phase. SEM results exhibited dense and homogeneous surfaces and enhanced surface grains with increased annealing temperature. The compositional formation of ZrO2 nanostructures were proved by electron dissipated x-ray and mapping analysis. Optical measuremets were strongly changed dependent on the grain size (GS).

Keywords

ZrO2 Optical constant Extinction coefficient Refractive index Reel dielectric constant

References

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Büyüklüğe Bağlı ZrO2 Nanoyapılarının Yapısal Parametrelerinin ve Optiksel Sabitlerinin Hesaplanması

Year 2024, Volume: 10 Issue: 1, 114 - 124, 30.04.2024

Gülsen Şahin Sultan Göktaş

Abstract

Bu çalışmada büyüklüğe bağlı zirkonyum dioksit (ZrO2) nanoyapılarının yapısal parametreleri ve optiksel sabitleri hesaplanmıştır. Parçacık boyutunun hesaplanan yapısal ve optiksel parametreler/sabitler üzerindeki etkisi araştırıldı. ZrO2 nanoyapıları kimyasal yolla üretildi. ZrO2 nanoyapılarının tane boyutunu değiştirmek için farklı tavlama sıcaklıkları (450-550 oC) uygulandı. Yapısal ve optiksel parametreleri/sabitleri hesaplamak için x-ışını kırınımı (XRD), taramalı elektron mikroskobu (SEM) ve ultraviyole/görünür bölge (UV-Vis) spektroskopisi ölçüm sonuçları kullanıldı. XRD ölçümü sonuçları, ZrO2 nanoyapılarının tetragonal (kübik) fazında kristalleştiğini gösterdi. SEM sonuçları, yoğun ve homojen yüzeyler ve artan tavlama sıcaklığıyla beraber yüzey tanelerinin büyüdüğünü sergiledi. ZrO2 nanoyapılarının bileşiksel oluşumu elektron dağılımlı x-ışını ve haritalama analizi ile kanıtlanmıştır. Optiksel ölçümler tane boyutuna (GS) bağlı olarak büyük ölçüde değişti.

Keywords

ZrO2 Optiksel sabit Yok olma katsayısı Kırılma indisi Reel dielektrik katsayısı

References

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  • [2] S. Goktas, A. Tumbul and A. Goktas, “Growth Technique–Induced Highly C-Axis-Oriented ZnO: Mn, ZnO: Fe and ZnO: Co Thin Films: A Comparison of Nanostructure, Surface Morphology, Optical Band Gap, and Room Temperature Ferromagnetism,” Journal of Superconductivity and Novel Magnetism, vol. 36, pp. 1875–1892, 2023. doi:10.1007/s10948-023-06630-4
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  • [5] C-Y. Lin, C-Y. Wu, C-Y. Wu, T-C. Lee, F-L. Yang, C. Hu and T-Y. Tseng, “Effect of top electrode material on resistive switching properties of ZrO2 film memory devices,” IEEE Electron Device Letters, vol. 28, no. 5, pp. 366–368, 2007. doi:10.1109/LED.2007.894652
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  • [8] L. Liu, C. Li, Y. Chen, X. Zhang, L. Li and Y. Wang, “Phase transformation of ZrO2 nanocrystals induced by Li+,” Materials Letters, vol. 79, pp. 75–77, 2012. doi:10.1016/j.matlet.2012.03.112
  • [9] S. Tekeli and U. Demir, “Colloidal processing, sintering and static grain growth behavior of alumina-doped cubic zirconia,” Ceramics International, vol. 31, no. 7, pp. 973-980, 2005. doi:10.1016/j.ceramint.2004.10.011
  • [10] S.K. Durrani, J. Akhtar, M. Ahmad and M.A. Hussain, “Synthesis and characterization of low density calcia stabilized zirconia ceramic for high temperature furnace application,” Materials Chemistry and Physics, vol. 100, no. 2–3, pp. 324-328, 2006. doi:10.1016/j.matchemphys.2006.01.010
  • [11] O. Bernard, A.M. Huntz, M. Andrieux, W. Seiler, V. Ji and S. Poissonnet, “Synthesis, structure, microstructure and mechanical characteristics of MOCVD deposited zirconia films,” Applied Surface Science, vol. 253, no. 10, pp. 4626-4640, 2007. doi:10.1016/j.apsusc.2006.10.025
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  • [15] V. S. Anitha, S. S. Lekshmy and K. Joy, “Effect of annealing temperature on optical and electrical properties of ZrO2–SnO2 nanocomposite thin films,” Journal of Materials Science: Materials in Electronics, vol. 24, pp. 4340–4345, 2013. doi:10.1007/s10854-013-1408-7
  • [16] A. Goktas, F. Aslan and İ.H. Mutlu, “Annealing effect on the characteristics of La0.67Sr0.33MnO3 polycrystalline thin films produced by the sol–gel dip-coating process,” Journal of Materials Science: Materials in Electronics, vol. 23, pp. 605–611, 2012. doi:10.1007/s10854-011-0448-0
  • [17] I. J. Berlin, S. S. Lekshmy, V. Ganesan, P.V. Thomas and K. Joy, “Effect of Mn doping on the structural and optical properties of ZrO2 thin films prepared by sol–gel method,” Thin Solid Films, vol. 550, pp. 199-205, 2014. doi:10.1016/j.tsf.2013.10.164
  • [18] A. Goktas, F. Aslan, A. Tumbul and S. Gunduz, “Tuning of structural, optical and dielectric constants by various transition metal doping in ZnO:TM (TM=Mn, Co, Fe) nanostructured thin films: A comparative study,” Ceramics International, vol. 43, no. 1, pp. 704-713, 2017. doi:10.1016/j.ceramint.2016.09.217
  • [19] A. Goktas, I. H. Mutlu and Y. Yamada, “Influence of Fe-doping on the structural, optical, and magnetic properties of ZnO thin films prepared by sol–gel method,” Superlattices and Microstructures, vol. 57, pp. 139-149, 2013. doi:10.1016/j.spmi.2013.02.010
  • [20] A. Méndez-López, O. Zelaya-Ángel, M. Toledano-Ayala, I. Torres-Pacheco, J. F. Pérez-Robles and Y. J. Acosta-Silva, “The Influence of Annealing Temperature on the Structural and Optical Properties of ZrO2 Thin Films and How Affects the Hydrophilicity,” Crystals, vol. 10, no. 6, pp. 454. 2020. doi:10.3390/cryst10060454
  • [21] H. Gencer, A. Goktas, M. Gunes, H.I. Mutlu and S. Atalay, “Electrical Transport and Magnetoresistance Properties of La0.67Ca0.33MnO3 Film Coated On Pyrex Glass Substrate,” International Journal of Modern Physics B, vol. 22, no. 05, pp. 497-506, 2008. doi:10.1142/S0217979208038776
  • [22] Y. Mansilla, M. D. Arce, C. González-Oliver, J. Basbus, H. Troiani and A. Serquis, “Characterization of stabilized ZrO2 thin films obtained by sol-gel method,” Applied Surface Science, vol. 569, pp. 150787, 2021. doi:10.1016/j.apsusc.2021.150787 [23] A. Göktaş, A. Tumbul, F. Aslan, “Grain size-induced structural, magnetic and magnetoresistance properties of Nd0.67Ca0.33MnO3 nanocrystalline thin films,” Journal of Sol-Gel Science and Technology, vol. 78, pp. 262–269, 2016. doi:10.1007/s10971-016-3960-0
  • [24] F. Mikailzade, F. Önal, M. Maksutoglu, M. Zarbali and A. Göktaş, “Structure and Magnetization of Polycrystalline La0.66Ca0.33MnO3 and La0.66Ba0.33MnO3 Films Prepared Using Sol-Gel Technique,” Journal of Superconductivity and Novel Magnetism, vol. 31, pp. 4141–4145, 2018. doi:10.1007/s10948-018-4683-y
  • [25] M. Boulouz, L. Martin, A. Boulouz and A. Boyer, “Effect of the dopant content on the physical properties of Y2O3–ZrO2 and CaO–ZrO2 thin films produced by evaporation and sputtering techniques,” Materials Science and Engineering: B, vol. 67, no. 3, pp. 122-131, 1999. doi:10.1016/S0921-5107(99)00338-4
  • [26] W.T. Tang, Z.F. Ying, Z.G. Hu, W.W. Li, J. Sun, N. Xu and J.D. Wu, “Synthesis and characterization of HfO2 and ZrO2 thin films deposited by plasma assisted reactive pulsed laser deposition at low temperature,” Thin Solid Films, vol. 518, no. 19, pp. 5442-5446, 2010. doi:10.1016/j.tsf.2010.04.012
  • [27] D. Tahir, E. Kyoung Lee, S. Kun Oh, H. Jae Kang, S. Heo, J. Gwan Chung, J. Cheol Lee and S. Tougaard, “Dielectric and optical properties of Zr silicate thin films grown on Si (100) by atomic layer deposition,” Journal of Applied Physics, vol. 106, no. 8, pp. 084108-14, 2009. doi:10.1063/1.3246612
  • [28] A. Goktas, F. Aslan, B. Yeşilata and İ. Boz, “Physical properties of solution processable n-type Fe and Al co-doped ZnO nanostructured thin films: Role of Al doping levels and annealing,” Materials Science in Semiconductor Processing, vol. 75, pp. 221-233, 2018. doi:10.1016/j.mssp.2017.11.033
  • [29] M. T. Soo, N. Prastomo, A. Matsuda, G. Kawamura, H. Muto, A. F. M. Noor, Z. Lockman and K. Y. Cheong, “Elaboration and characterization of sol–gel derived ZrO2 thin films treated with hot water,” Applied Surface Science, vol. 258, no. 13, pp. 5250-5258, 2012. doi:10.1016/j.apsusc.2012.02.008
  • [30] S. Chang and R. Doong, “The Effect of Chemical States of Dopants on the Microstructures and Band Gaps of Metal-Doped ZrO2 Thin Films at Different Temperatures,” The Journal of Physical Chemistry B, vol. 108, no. 46, pp. 18098-18103, 2004. doi:10.1021/jp047440n
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Details

Primary Language English
Subjects Classical Physics (Other)
Journal Section Research Articles
Authors

Gülsen Şahin 0000-0003-4891-041X

Sultan Göktaş 0009-0000-7084-9710

Early Pub Date April 6, 2024
Publication Date April 30, 2024
Submission Date October 23, 2023
Acceptance Date March 1, 2024
Published in Issue Year 2024 Volume: 10 Issue: 1

Cite

IEEE G. Şahin and S. Göktaş, “Calculation of Structural Parameters and Optical Constants of Size Dependent ZrO2 Nanostructures”, GJES, vol. 10, no. 1, pp. 114–124, 2024.
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